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Laboratory Services

XRF ANALYSIS | HYDRATION ANALYSIS | OTHER SERVICES

LABORATORY SERVICES
The bulk of our laboratory services are geared towards archaeometric analyses of artifacts made of obsidian and, to a lesser degree, basalt. Unless you choose our discounted Basic Report option, each project is returned with a brief written report and detailed data tables (suitable for use as a standalone appendix). Individual descriptions of obsidian sources identified through trace element studies are provided through our companion website at www.sourcecatalog.com.

All projects are returned with an CD containing (1) a speadsheet with all analytical results, (2) graphics files of any figures that appear in your report, and (3) copies of any Adobe Acrobat files that were produced as part of your project (including the overall final report). For a downloadable sample of our reports, click HERE. Standard shipping (UPS, Fedex, or Certified/Delivery Confirmation mail) of artifacts and results is included with all projects.

To submit samples for XRF and/or obsidian hydration analysis, please use the Adobe Acrobat sample submission form provided by Northwest Research. Alternatively you can print out the web sample submission form, or we'll be glad to mail, fax, or email you a copy. All samples should be sent to the lab in Corvallis, Oregon. For additional details on sending samples to the lab for analysis, click on the How To tab at the top of this page.

XRF ANALYSIS OF OBSIDIAN AND BASALT ARTIFACTS
Northwest Research owns and operates a Spectrace 5000 energy-dispersive X-ray fluorescence (EDXRF) spectrometer that is used to determine the trace and minor element composition of archaeological and geological specimens. Using a custom database management system, the results of the trace element analyses are compared with our extensive geologic source reference collection, allowing us to identify the geologic sources of obsidian and basalt artifacts. The patterns of source use that are revealed by the provenance analysis of artifacts can then be used to explore prehistoric procurement and exchange systems and may be used to indirectly examine a number of other prehistoric cultural processes.

Our Spectrace 5000 XRF spectrometer

Left to right: From artifact to analysis.

The process of XRF trace element analysis is entirely nondestructive but is limited to obsidian and basalt artifacts with a minimum diameter of no less than about 10 mm and a thickness of no less than 1.5 mm. Larger specimens are preferred for analysis and should be selected whenever possible.

CLICK HERE FOR ADDITIONAL DETAILS ABOUT XRF ANALYSIS

HYDRATION ANALYSIS OF OBSIDIAN ARTIFACTS

Obsidian hydration rim found on an artifact from Easter Island.

When a surface of freshly-flaked obsidian is exposed to the air, water is slowly absorbed into the surface of the artifact, leaving a narrow hydration rim that is visible under a microscope. The thickness of the rim depends, in part, on the age of an artifact, and provides researchers with the opportunity to directly determine the approximate age of its manufacture.

Small cut left by hydration analysis preparation

A thin slice (1-1.5 mm wide) of obsidian has been removed from the edge of the projectile
point above as part of the process of measuring the hydration rim on the artifact.

As is visible in the image above, the process of slide preparation is slightly destructive. A thin slice of glass is first carefully removed from the edge of an artifact. This thin wafer is fastened to a slide, ground to a thickness of about 30-50 microns, and is examined with a petrographic microscope. The hydration rim that has formed on the surface of the artifact can then be accurately measured to a precision of approximately +/- 0.2 microns.

CLICK HERE FOR ADDITIONAL DETAILS ABOUT OBSIDIAN HYDRATION ANALYSIS

OTHER LAB SERVICES
  • Discounted Basic Report Special. We offer a flat 10% discount for all analytical services that do not require a complete final report. For the Basic Report, you'll still get publication-quality data tables, spreadsheets with your data, and full lab and web support. For those of you that don't need a polished final report for your shelf or special studies appendix, this is a good way to stretch your research budget.

  • Rapid Turnaround. In a serious hurry? For an extra 35%, we'll drop everything else, forsake our families and friends, and focus on your job. Within two weeks, you'll have a copy of the results faxed or emailed to you. The extra charge covers overtime and strained relationships with our families and other customers. For obvious reasons, a two week turnaround may not be practical for rather large jobs. If you're absolutely counting on the rapid turnaround to meet a critical project deadline, it's essential to contact us in advance.

  • Source Investigations. An understanding of the geochemical variability and geographic distribution of obsidian sources is a fundamental component of any obsidian characterization or procurement investigation. Geochemical data from a wide variety of published and unpublished sources can also be used to examine large-scale distribution and spatial patterns of prehistoric use (see the trend surface map below). Depending on your needs and budget, we can perform geochemical inventories and/or geoarchaeological studies of sources from the smallest to largest scales.

    Trend surface analysis depicting prehistoric source use of Silver Lake/Sycan Marsh obsidian source

    Trend surface analysis of obsidian XRF data for artifacts correlated
    with the Silver Lake/Sycan Marsh source in Oregon.

    Any of the new services described above can requested by adding them to the "Other" section of our standard Sample Submission form. Be sure to specify which service you are interested in on the submission form or in a cover letter.

  • Back to the Obsidian Lab Home Page


    Last Updated: 03/07/2007
    Northwest Research Obsidian Studies Laboratory